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derrickman
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Measuring Lead Hardness...
Aug 4th, 2016 at 10:45am
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What is the preference for determining lead alloy/hardness?
I've been using the Cabin Tree tool for some time. I question it however because when I test certified 1/20 alloy it consistently reads it as softer than advertised.  To further confuse matters, sometimes I'll test both ends of a flat nose bullet & get two completely different results. 
I'm thinking there should be a more definitive tool out there. I'd like to know what the pros use; I've only been at this for 20 years & still learning.
Thanks in advance.
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KAF
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Re: Measuring Lead Hardness...
Reply #1 - Aug 4th, 2016 at 11:03am
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I use the Lee hardness measure.
You have to be steady and have good light on the dent to measure it.  But I have come up with good readings compared to a control measurement from metalugical charts.

I/ve want to use an old mocroscope to mount the magnifier on/in to make it easier.

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frnkeore
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Re: Measuring Lead Hardness...
Reply #2 - Aug 4th, 2016 at 12:34pm
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This is the method that I use. It comes from the NRA's Cast Bullet Manual. It is for measuring ingots and the results are extremely accurate when compared to a certified 20/1 ingot and other accurate testers. Not all available testers are accurate.

You only need a known, pure lead sample and a steel ball, between 1/2"
and 1" in diameter.

You place the ball, between the pure lead sample and any cast ingot you want to test. You apply enough pressure to the above "Sandwich" to make a impression, no larger than 1/4 of the ball diameter and no deeper than 1/4 of the ingot thickness. The test area should be filed flat as any test area should be, for all testers. You then measure the impressions and run this formula on  the measurements:

"pure lead diameter / sample diameter, squared, times 5 (hardness of pure lead)"

There is a very long thread over on CBA's site, testing many different hardness testers, including Lee and Cabine. NRA's method is perfect, up to 20/1 but, he didn't use the prescribed ball diameter, his was 10mm, not the minimum of 1/2" diameter.

I've used this method since I learned about it in the 80's. I use a 5/8 ball and it gives accurate reading on 20/1, WW/2% tin and #2 alloy.

The price is just $0 to a few bucks.
 
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« Last Edit: Aug 4th, 2016 at 12:40pm by frnkeore »  

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JLouis
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Re: Measuring Lead Hardness...
Reply #3 - Aug 4th, 2016 at 1:17pm
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I think some of the errors one sees in there testers is when they are making up there own alloy and lets say for example its 20-1. Common thought is you take 20lbs. of pure lead and add 1lb. of pure tin of which is not exactly correct as you end up with 21lbs. The proportions of lead and tin need to equate to 20lbs. and this would be enough to provide the false readings some are incurring on their various alloy testers.

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BP
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Re: Measuring Lead Hardness...
Reply #4 - Aug 4th, 2016 at 1:42pm
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JLouis wrote on Aug 4th, 2016 at 1:17pm:
I think some of the errors one sees in there testers is when they are making up there own alloy and lets say for example its 20-1. Common thought is you take 20lbs. of pure lead and add 1lb. of pure tin of which is not exactly correct as you end up with 21lbs. The proportions of lead and tin need to equate to 20lbs. and this would be enough to provide the false readings some are incurring on their various alloy testers.

JLouis

So how do you do it, JLouis?
20:1 is 20 parts of something mixed with 1 part of something else, giving a total of 21 parts.
Are you proportioning your mix by by chemical molar weight or by volume, or by ... ?
  

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frnkeore
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Re: Measuring Lead Hardness...
Reply #5 - Aug 4th, 2016 at 1:44pm
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20/1 is and has always been 20 parts lead and one part tin. Therefore the tin is 1/21 of the mix by weight or 4.76% tin.

20/1 is not a total of 20 parts, which is 19/1 or 5% tin, as many think. The hardness is 10 BHN for 20/1 and 10.05 BHN for 19/1

But, non of the available hardness tester are sensitive enough to measure the difference, accurately.

My 22/1 (4.17%) alloy has a BHN of 9.80, you would also be hard pressed to get that BHN exact with any tester also.

The available testers that you have to measure the indent are VERY subseptable to errors in reading the indent, .002 can make a real difference. Not everyone can read the indents accurately. Shadows, parellax and rounded edges can cause, at least that much error.

Frank
« Last Edit: Aug 4th, 2016 at 2:50pm by frnkeore »  

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Re: Measuring Lead Hardness...
Reply #6 - Aug 4th, 2016 at 2:15pm
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Just to comment on the mixes---how many rifles can tell the difference in the alloy from 20:1 over John's 19:1? 
I don't test by hardness, anyhow, but the question has been one I"ve wondered about for years.
I had an old mentor way back when- he didn't think much about it, and he was a fine caster and shooter, both. Mixed his alloy by eye- or at least some innate  sense of heat, casting ease or whatever.
  
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Re: Measuring Lead Hardness...
Reply #7 - Aug 4th, 2016 at 2:19pm
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BP I do it the way I was taught to come up with a true 20-1 alloy by proportioning. I could be wrong but through my conversations with RotoMetals from what I understand it is also the same method they use for producing thier various alloys. But it surely is not worth arguing over if one feels other wise as it is much simpliar to just continue on doing what you think is correct and works best for you.

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Re: Measuring Lead Hardness...
Reply #8 - Aug 4th, 2016 at 2:31pm
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JLouis,
Keep on doing whatever you were taught if it works for you.
Math is math.
Example: If I'm walking through a car lot, and I count a total of 20 Chevys, and one Ford, I have 20/1 (Chevy/Ford), with a total of 21 vehicles.
  

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Re: Measuring Lead Hardness...
Reply #9 - Aug 4th, 2016 at 2:35pm
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CF I don't think how one chooses to make his alloy has any real bearing and surely not enough to argue over. But I do strongly feel each individual rifle performs its best by the using the correct bullet hardness and it can change when changing to other various bullet designs in the same rifle. Not based on opinion it is simply another one of those varibles that I have taken the time to prove only to myself.

JLouis
  

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Re: Measuring Lead Hardness...
Reply #10 - Aug 4th, 2016 at 2:46pm
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the "xx:Y  or xx/y has always seemed to me terms that lead to confusion.
For that reason, for my own designating of alloy I use the term
for example: 
 
20+1   or 19+1 lead plus tin   
or in my case mostly:     9+1 ww/lino
Much more clear what we have that way
beltfed/arnie
  
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Re: Measuring Lead Hardness...
Reply #11 - Aug 4th, 2016 at 2:53pm
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Not arguing- just want to hear if rifles in general are so fussy as to need a precise alloy- or if one almost, but not exactly, the same will behave as well. Most rifles,not just your obviously fussy one.
Nothing wrong with your way, keep up the good work if ya like it that way. But, did you really see if the other slightly different alloy worked? I can see where a big swing in alloy may have consequences, but a tiny one is like measuring the amount of milk in your pancake batter with a triple beam scale. Not needed there- is it any difference with lead? In this case mentioned earlier the difference is 4.76% compared to 5%. If the ingredients are pure to begin with.
  
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JLouis
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Re: Measuring Lead Hardness...
Reply #12 - Aug 4th, 2016 at 3:02pm
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Beltfed I have seen shoes tied on in various manners over the years and the end result is to simply have the shoes stay on and not what method is correct or incorrect but whats the easiest way for one to do it. The same goes for the way one chooses to make his alloy, as long as the bullet likes the end hardness and it is easily repeatable for the person making it nothing else really matters.

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Re: Measuring Lead Hardness...
Reply #13 - Aug 4th, 2016 at 3:08pm
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I guess the real measure of proof of anything, is the ability to shoot 250's in a actual match. I'm not quite there, myself. My scores are 248's and 249's at Spokane and only .463 and 1.288, 5 and ten shot groups here. You may also note that many of the 250 shooters use 24 - 25/1.

I've tried everything from 30/1 to 16/1 but, I keep coming back to 22 - 20/1. I only shoot spitzers and in that range, they seem to hold their shape.

But, this thread is REALLY about hardness testing and for those with testers, you'll find that you have to test, at least 3 times and average your tests. It's not uncommon to get readings of +/- .5 hardnest on the same test sample, no matter how well you think your lead is mixed and how much of any alloy is in it.

For our sport, if you know the lead and tin that you put into the mix, you really have no need to test it's hardness. But, if you get lead and tin from unknown sources, it's best to test it. Especially if you use Pewter as your tin. But, again, your test results will have to be averaged and will not, probably be any closer to the actual hardness tha, about +/- .2, at best.

One more thing about unknow sources, if you have any Arsinc or antimony in it, it will age harden and if you store your bullets for more than 1 week, before you shoot , you need to re-test them, to make sure they stay the same hardness. At 2 weeks, most of those alloys reach their hardest point.

Frank
« Last Edit: Aug 4th, 2016 at 4:02pm by frnkeore »  

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derrickman
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Re: Measuring Lead Hardness...
Reply #14 - Aug 4th, 2016 at 3:14pm
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Someone once told me that he once filled his melting pot with certified 1/20 alloy & then cast his bullets for silhouette. They all weighed xxx grs. so after that he used unknown alloy but always added either pure lead or tin to get his bullets to weigh xxx grs same as what he got with 1/20 alloy. He seemed content with his lot in life.
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